Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum
The cell wall composition of Japanese plums (Prunus salicina) at six developmental stages was previously evaluated (Ponce et al., J. Agric. Food Chem. 2010, 58, 2562-2570). This fruit is an interesting source of pectins, polysaccharides of valuable functionality for pharmaceutical and food formulati...
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todo:paper_01448617_v89_n1_p230_Basanta2023-10-03T14:59:50Z Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum Basanta, M.F. Ponce, N.M.A. Rojas, A.M. Stortz, C.A. Flow behavior Japanese plum Pectins Viscosity Water extraction Aqueous extraction Average molecular weight Boiling water Cell wall composition Degree of methylations Developmental stage Extraction time Flow behaviors High viscosities Hot water Japanese plum Pectins Rheological characteristics Room temperature Water extraction Water solutions Alkylation Molecular weight Viscosity Solvent extraction Prunus Prunus domestica Prunus salicina pectin plant extract water cell wall chemistry flow kinetics fruit Prunus size exclusion chromatography temperature time Cell Wall Chromatography, Gel Fruit Pectins Plant Extracts Prunus Rheology Temperature Time Factors Water The cell wall composition of Japanese plums (Prunus salicina) at six developmental stages was previously evaluated (Ponce et al., J. Agric. Food Chem. 2010, 58, 2562-2570). This fruit is an interesting source of pectins, polysaccharides of valuable functionality for pharmaceutical and food formulations. In the present work it was investigated how the different conditions for the aqueous extraction of pectins from Japanese plums affect the yield as well as their chemical and rheological characteristics. It has been determined that extraction with water at room temperature for periods longer than 2 h did not produce additional increment of yield (12%) but decreased the average molecular weights of the extracted pectins. Pectins with a degree of methylation ≈40% with high viscosity in water and with adequate molecular weights (≈72,000) were obtained. Conversely, utilization of boiling water for extraction increased considerably the yields (33-38%) but the extracted pectins showed significant lower viscosity in water in spite of their higher molecular weights. The poorer thickening ability was associated to the lower proportion of arabinose residues present in the hairy regions of the pectin macromolecules extracted by hot water, which led the polymers to interact more transiently in a 2% w/v water solution. © 2012 Elsevier Ltd. All rights reserved. Fil:Basanta, M.F. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Fil:Rojas, A.M. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Fil:Stortz, C.A. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. JOUR info:eu-repo/semantics/openAccess http://creativecommons.org/licenses/by/2.5/ar http://hdl.handle.net/20.500.12110/paper_01448617_v89_n1_p230_Basanta |
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Universidad de Buenos Aires |
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I-28 |
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R-134 |
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Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA) |
| topic |
Flow behavior Japanese plum Pectins Viscosity Water extraction Aqueous extraction Average molecular weight Boiling water Cell wall composition Degree of methylations Developmental stage Extraction time Flow behaviors High viscosities Hot water Japanese plum Pectins Rheological characteristics Room temperature Water extraction Water solutions Alkylation Molecular weight Viscosity Solvent extraction Prunus Prunus domestica Prunus salicina pectin plant extract water cell wall chemistry flow kinetics fruit Prunus size exclusion chromatography temperature time Cell Wall Chromatography, Gel Fruit Pectins Plant Extracts Prunus Rheology Temperature Time Factors Water |
| spellingShingle |
Flow behavior Japanese plum Pectins Viscosity Water extraction Aqueous extraction Average molecular weight Boiling water Cell wall composition Degree of methylations Developmental stage Extraction time Flow behaviors High viscosities Hot water Japanese plum Pectins Rheological characteristics Room temperature Water extraction Water solutions Alkylation Molecular weight Viscosity Solvent extraction Prunus Prunus domestica Prunus salicina pectin plant extract water cell wall chemistry flow kinetics fruit Prunus size exclusion chromatography temperature time Cell Wall Chromatography, Gel Fruit Pectins Plant Extracts Prunus Rheology Temperature Time Factors Water Basanta, M.F. Ponce, N.M.A. Rojas, A.M. Stortz, C.A. Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum |
| topic_facet |
Flow behavior Japanese plum Pectins Viscosity Water extraction Aqueous extraction Average molecular weight Boiling water Cell wall composition Degree of methylations Developmental stage Extraction time Flow behaviors High viscosities Hot water Japanese plum Pectins Rheological characteristics Room temperature Water extraction Water solutions Alkylation Molecular weight Viscosity Solvent extraction Prunus Prunus domestica Prunus salicina pectin plant extract water cell wall chemistry flow kinetics fruit Prunus size exclusion chromatography temperature time Cell Wall Chromatography, Gel Fruit Pectins Plant Extracts Prunus Rheology Temperature Time Factors Water |
| description |
The cell wall composition of Japanese plums (Prunus salicina) at six developmental stages was previously evaluated (Ponce et al., J. Agric. Food Chem. 2010, 58, 2562-2570). This fruit is an interesting source of pectins, polysaccharides of valuable functionality for pharmaceutical and food formulations. In the present work it was investigated how the different conditions for the aqueous extraction of pectins from Japanese plums affect the yield as well as their chemical and rheological characteristics. It has been determined that extraction with water at room temperature for periods longer than 2 h did not produce additional increment of yield (12%) but decreased the average molecular weights of the extracted pectins. Pectins with a degree of methylation ≈40% with high viscosity in water and with adequate molecular weights (≈72,000) were obtained. Conversely, utilization of boiling water for extraction increased considerably the yields (33-38%) but the extracted pectins showed significant lower viscosity in water in spite of their higher molecular weights. The poorer thickening ability was associated to the lower proportion of arabinose residues present in the hairy regions of the pectin macromolecules extracted by hot water, which led the polymers to interact more transiently in a 2% w/v water solution. © 2012 Elsevier Ltd. All rights reserved. |
| format |
JOUR |
| author |
Basanta, M.F. Ponce, N.M.A. Rojas, A.M. Stortz, C.A. |
| author_facet |
Basanta, M.F. Ponce, N.M.A. Rojas, A.M. Stortz, C.A. |
| author_sort |
Basanta, M.F. |
| title |
Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum |
| title_short |
Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum |
| title_full |
Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum |
| title_fullStr |
Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum |
| title_full_unstemmed |
Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum |
| title_sort |
effect of extraction time and temperature on the characteristics of loosely bound pectins from japanese plum |
| url |
http://hdl.handle.net/20.500.12110/paper_01448617_v89_n1_p230_Basanta |
| work_keys_str_mv |
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