Viscosity and thermal evolution of density and wetting angle of a commercial glaze by means of hot stage microscopy

In the present work we attempt to describe the results of the thermal behavior analysis of a commercial glaze obtained in a thermal microscope developed by the research group. At the same time, the density and the wetting angle of the glaze with an alumina surface was evaluated. Particularly the sin...

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Autores principales: Stábile, Franco Matías, Picicco, Martiniano, Serra, María Florencia, Rafti, Matías, Suárez, Gustavo, Rendtorff Birrer, Nicolás Maximiliano
Formato: Articulo
Lenguaje:Inglés
Publicado: 2015
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Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/123846
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id I19-R120-10915-123846
record_format dspace
institution Universidad Nacional de La Plata
institution_str I-19
repository_str R-120
collection SEDICI (UNLP)
language Inglés
topic Química
Glass
hot stage microscopy
viscosity
wetting angle
spellingShingle Química
Glass
hot stage microscopy
viscosity
wetting angle
Stábile, Franco Matías
Picicco, Martiniano
Serra, María Florencia
Rafti, Matías
Suárez, Gustavo
Rendtorff Birrer, Nicolás Maximiliano
Viscosity and thermal evolution of density and wetting angle of a commercial glaze by means of hot stage microscopy
topic_facet Química
Glass
hot stage microscopy
viscosity
wetting angle
description In the present work we attempt to describe the results of the thermal behavior analysis of a commercial glaze obtained in a thermal microscope developed by the research group. At the same time, the density and the wetting angle of the glaze with an alumina surface was evaluated. Particularly the sintering temperature, the sphere, semi-sphere and fusion temperatures were also determined. These present characteristic viscosities. Afterward, by means of the de Vogel-Fulcher-Tammann equation, the viscosity as a function of temperature was estimated. In the first part the developed equipment is described together with the image analysis carried out for the in-situ cylindrical samples (2,5 mm of height and diameter). The thermal cycle was up to 1200ºC with a heating rate of 5ºC/min. The developed equipment presents the following characteristics: some problems with the temperature evaluation, it was slightly affected by air currents and difficulties for achieving an adequate parallelism. On the other hand, the potentialities of the equipment for development and study of the thermal behavior of glasses was established.
format Articulo
Articulo
author Stábile, Franco Matías
Picicco, Martiniano
Serra, María Florencia
Rafti, Matías
Suárez, Gustavo
Rendtorff Birrer, Nicolás Maximiliano
author_facet Stábile, Franco Matías
Picicco, Martiniano
Serra, María Florencia
Rafti, Matías
Suárez, Gustavo
Rendtorff Birrer, Nicolás Maximiliano
author_sort Stábile, Franco Matías
title Viscosity and thermal evolution of density and wetting angle of a commercial glaze by means of hot stage microscopy
title_short Viscosity and thermal evolution of density and wetting angle of a commercial glaze by means of hot stage microscopy
title_full Viscosity and thermal evolution of density and wetting angle of a commercial glaze by means of hot stage microscopy
title_fullStr Viscosity and thermal evolution of density and wetting angle of a commercial glaze by means of hot stage microscopy
title_full_unstemmed Viscosity and thermal evolution of density and wetting angle of a commercial glaze by means of hot stage microscopy
title_sort viscosity and thermal evolution of density and wetting angle of a commercial glaze by means of hot stage microscopy
publishDate 2015
url http://sedici.unlp.edu.ar/handle/10915/123846
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