Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds
3β-Hydroxy-5-cholenic acid was synthesized from 3β-hydroxy-5-pregnen-20-one in nine steps. The procedure would permit the labelling of C-22, C-23, and/or C-24 of the bile-acid side chain by choice of the appropriate labelled reagent. © 1977.
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| Acceso en línea: | http://hdl.handle.net/20.500.12110/paper_00224731_v8_n1_p69_Burton |
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todo:paper_00224731_v8_n1_p69_Burton2023-10-03T14:33:12Z Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds Burton, G. Gros, E.G. carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols 3β-Hydroxy-5-cholenic acid was synthesized from 3β-hydroxy-5-pregnen-20-one in nine steps. The procedure would permit the labelling of C-22, C-23, and/or C-24 of the bile-acid side chain by choice of the appropriate labelled reagent. © 1977. Fil:Burton, G. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Fil:Gros, E.G. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. JOUR info:eu-repo/semantics/openAccess http://creativecommons.org/licenses/by/2.5/ar http://hdl.handle.net/20.500.12110/paper_00224731_v8_n1_p69_Burton |
| institution |
Universidad de Buenos Aires |
| institution_str |
I-28 |
| repository_str |
R-134 |
| collection |
Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA) |
| topic |
carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols |
| spellingShingle |
carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols Burton, G. Gros, E.G. Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds |
| topic_facet |
carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols |
| description |
3β-Hydroxy-5-cholenic acid was synthesized from 3β-hydroxy-5-pregnen-20-one in nine steps. The procedure would permit the labelling of C-22, C-23, and/or C-24 of the bile-acid side chain by choice of the appropriate labelled reagent. © 1977. |
| format |
JOUR |
| author |
Burton, G. Gros, E.G. |
| author_facet |
Burton, G. Gros, E.G. |
| author_sort |
Burton, G. |
| title |
Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds |
| title_short |
Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds |
| title_full |
Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds |
| title_fullStr |
Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds |
| title_full_unstemmed |
Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds |
| title_sort |
synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds |
| url |
http://hdl.handle.net/20.500.12110/paper_00224731_v8_n1_p69_Burton |
| work_keys_str_mv |
AT burtong synthesisof3bhydroxy5cholenicacidfrom3bhydroxy5pregnen20oneaimedatthepreparationoflabelledsteroidcompounds AT groseg synthesisof3bhydroxy5cholenicacidfrom3bhydroxy5pregnen20oneaimedatthepreparationoflabelledsteroidcompounds |
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