Carboxylation treatment of multiwalled carbon nanotubes monitored by infrared and ultraviolet spectroscopies and scanning probe microscopy

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The effect of acid treatment on multiwalled carbon nanotubes (MWCNTs) was investigated through analysis of their morphologies followed by atomic force microscopy (AFM). The chemical changes were monitored by Fourier transform infrared (FTIR) and ultraviolet (UV/Vis) spectrophotometries. Treatments w...

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Detalles Bibliográficos
Autor principal: Goyanes, Silvia Nair
Otros Autores: Rubiolo, G.R, Salazar, A., Jimeno, A., Corcuera, M.A, Mondragon, Iñaki
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 2007
Acceso en línea:Registro en Scopus
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Biblioteca Central Dr. Luis F. Leloir (FCEN) de Universidad de Buenos Aires
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100 1 |a Goyanes, Silvia Nair 
245 1 0 |a Carboxylation treatment of multiwalled carbon nanotubes monitored by infrared and ultraviolet spectroscopies and scanning probe microscopy 
260 |c 2007 
270 1 0 |m Mondragon, I.; 'Materials + Technologies' Group, Escuela Univ Politécnica/Unibertsitate Eskola Politeknikoa, Dpto Ingeniería Química y M Ambiente, Pza Europa 1, 20018 Donostia-San Sebastián, Spain; email: inaki.mondragon@ehu.es 
504 |a Meincke, O., Kaempfer, D., Weickmann, H., Friedrich, C., Vathauer, M., Warth, H., (2004) Polymer, 45, p. 739 
504 |a Ruoff, R.S., Lorents, D.C., (1995) Carbon, 33, p. 925 
504 |a Salvetat-Delmotte, J.P., Rubio, A., (2002) Carbon, 40, p. 1729 
504 |a Breton, Y., Desarmot, G., Salvetat, J.P., Delpeux, S., Sinturel, C., Beguin, F., Bonnamy, S., (2004) Carbon, 42, p. 1027 
504 |a Lau, K.T., Shi, S.Q., Cheng, H.M., (2003) Comput. Sci. Tech., 63, p. 1161 
504 |a Wang, Z., Liu, J., Liang, Q., Wang, Y., Luo, G., (2002) The Analyst, 127, p. 653 
504 |a Kim, J.K., Shin, T.S., Choi, H.D., Kwon, J.H., Chung, Y., Yonn, H.G., (2005) Carbon, 43, p. 23 
504 |a O ́Connell, M.J., Boul, P., Ericson, L.M., Huffman, C., Wang, Y., Haroz, E., Kuper, C., Smalley, R.D., (2001) Chem. Phys. Lett., 342, p. 265 
504 |a Choi, H.J., Park, S.J., Kim, S.T., Jhon, M.S., (2005) Diamond Relat. Mater., 14, p. 766 
504 |a Sung, J.H., Kim, H.S., Jin, H.-J., Choi, H.J., Chin, I.-J., (2004) Macromolecules, 37, p. 9899 
504 |a Lin, Y., Rao, M., Sadanadan, B., Kenik, E.A., Sun, Y.P., (2003) J. Phys. Chem., B, 106, p. 1294 
504 |a Dettlaff-Weglikowska, U., Benoit, J.M., Chiu, P.W., Graupner, R., Lebedkin, S., Roth, S., (2002) Curr. Appl. Phys., 2, p. 497 
504 |a Kong, H., Gao, C., Yan, D., (2004) J. Mater. Chem., 14, p. 1401 
504 |a Qin, S., Qin, D., Ford, W.T., Resasco, D.E., Herrera, J.E., (2004) J. Am. Chem. Soc., 126, p. 170 
504 |a Zhao, B., Brittain, W.J., (2000) Prog. Polym. Sci., 25, p. 677 
504 |a Wang, Y., Iqbal, Z., Malhotra, S.V., (2005) Chem. Phys. Lett., 402, p. 96 
504 |a Liu, J., Rinzler, A.G., Dai, H., Hafner, J.H., Bradley, R.K., Boul, P.J., Lu, A., Smalley, R.E., (1998) Science, 280, p. 1253 
504 |a Dujardin, E., Ebbesen, T.W., Krishnan, A., Treacy, M.M.J., (1998) Adv. Mater., 10, p. 611 
504 |a Hill, D.E., Lin, Y., Rao, A.M., Allard, L.F., Sun, Y.P., (2002) Macromolecules, 35, p. 9466 
504 |a Li, S., Qin, Y., Shi, J., Guo, Z.X., Li, Y., Zhu, D., (2005) Chem. Mater., 17, p. 130 
504 |a Eitan, A., Jiang, K., Dukes, D., Andrews, R., Schadler, L.S., (2003) Chem. Mater., 15, p. 3198 
504 |a Sun, Y.P., Zhou, B., Henbest, K., Fu, K., Huang, W., Lin, Y., Taylor, S., Carroll, D.L., (2002) Chem. Phys. Lett., 351, p. 349 
504 |a Chen, J., Hamon, M.A., Hu, H., Chen, Y., Rao, A.M., Eklund, P.C., Haddon, R.D., (1998) Science, 282, p. 95 
504 |a Zhang, J., Zou, H., Qing, Q., Yang, Y., Li, Q., Liu, Z., Guo, X., Du, Z., (2003) J. Phys. Chem., B, 107, p. 3712 
504 |a Kyotani, T., Nakazaki, S., Xu, W.H., Tomita, A., (2001) Carbon, 39, p. 771 
504 |a Burghard, M., (2005) Surf. Sci. Rep., 58, p. 1 
504 |a Liu, Y., Gao, L., (2005) Carbon, 43, p. 47 
504 |a Ramesh, B.P., Blau, W.J., Tyagi, P.K., Misra, D.S., Ali, N., Gracio, J., Cabral, G., Titus, E., (2006) Thin Solid Films, 494, p. 128 
504 |a Shaffer, M.S.P., Fan, X., Windle, A.H., (1998) Carbon, 36, p. 1603 
504 |a Strano, M.S., Dyke, C.A., Usrey, M.L., Barone, P.W., Allen, M.J., Shan, H., Kittrell, C., Smalley, R.E., (2003) Science, 301, p. 1519 
504 |a Chiang, I.W., Brinson, B.E., Huang, A.Y., Willis, P.A., Bronikowski, M.J., Margrave, J.L., Smalley, R.E., Hauge, R.H., (2001) J. Phys. Chem., B, 105, p. 8297 
504 |a Chiang, I.W., Brinson, B.E., Smalley, R.E., Margrave, J.L., Hauge, R.H., (2001) J. Phys. Chem., B, 105, p. 1157 
504 |a Zhao, J., Park, H., Han, J., Lu, J.P., (2004) J. Phys. Chem., B, 108, p. 4227 
504 |a Ajayan, P.M., (1999) Chem. Rev., 99, p. 1787 
504 |a Tsang, S.C., Harris, P.J.F., Green, M.L.H., (1993) Nature, 362, p. 520 
506 |2 openaire  |e Política editorial 
520 3 |a The effect of acid treatment on multiwalled carbon nanotubes (MWCNTs) was investigated through analysis of their morphologies followed by atomic force microscopy (AFM). The chemical changes were monitored by Fourier transform infrared (FTIR) and ultraviolet (UV/Vis) spectrophotometries. Treatments with nitric acid as well as with a mixture of nitric and sulfuric acids (1:3 by volume) were analyzed. Both acid treatments applied during a short ultrasonication time do not show any relevant effect. However, an additional peak can be observed at 1200 cm- 1 in the FTIR spectrum of the MWCNTs treated with the acid mixture after 2 h but their UV/Vis spectrum did not change. These results could indicate that new C-O groups appear in the open ends of the nanotubes without modifying the structure of their sidewalls. When the treatment with the acid mixture was prolonged, the sidewall of the nanotubes began to be destroyed up to their nearly complete destruction as observed by both UV/Vis and AFM. The results reported in this work show that three simple and quick techniques can help to control the carboxylation process often carried out before the functionalization of MWCNTs. © 2006 Elsevier B.V. All rights reserved.  |l eng 
536 |a Detalles de la financiación: Ministerio de Educación y Cultura, MAT2005-06530 
536 |a Detalles de la financiación: Agencia Nacional de Promoción Científica y Tecnológica 
536 |a Detalles de la financiación: Universidad de Buenos Aires 
536 |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas 
536 |a Detalles de la financiación: Funding for this work was provided by “Ministerio de Educación y Ciencia” (Spain) through Grant MAT2005-06530, Gobierno Vasco/Eusko Jaurlaritza and Diputación de Gipuzkoa — Programa ETORTEK/NANOTRON, and NANOFUN-POLY Network of Excellence as well as Universidad de Buenos Aires, Consejo Nacional de Investigaciones Científicas y Técnicas, Agencia Nacional de Promoción Científica y Tecnológica, Argentina. 
593 |a Laboratorio de Polímeros y Materiales Compuestos, Dep Física, FCEN-UBA. Ciudad Universitaria, Pab. 1, C1428EGA Buenos Aires, Argentina 
593 |a Consejo Nacional de Investigaciones Científicas y Tecnológicas, CONICET, Argentina 
593 |a Unidad de Actividad Materiales, CNEA, Av Gral. Paz 1499, San Martin, 1650 Buenos Aires, Argentina 
593 |a 'Materials + Technologies' Group, Escuela Univ Politécnica/Unibertsitate Eskola Politeknikoa, Dpto Ingeniería Química y M Ambiente, Pza Europa 1, 20018 Donostia-San Sebastián, Spain 
690 1 0 |a CHARACTERIZATION 
690 1 0 |a CHEMICAL TREATMENT 
690 1 0 |a MULTIWALLED CARBON NANOTUBES (MWCNTS) 
690 1 0 |a SCANNING PROBE TECHNIQUES 
690 1 0 |a SPECTROPHOTOMETRY 
690 1 0 |a ATOMIC FORCE MICROSCOPY 
690 1 0 |a CARBOXYLATION 
690 1 0 |a CHARACTERIZATION 
690 1 0 |a FOURIER TRANSFORM INFRARED SPECTROSCOPY 
690 1 0 |a INFRARED SPECTROSCOPY 
690 1 0 |a ULTRAVIOLET SPECTROPHOTOMETERS 
690 1 0 |a CHEMICAL TREATMENT 
690 1 0 |a MULTIWALLED CARBON NANOTUBES (MWCNT) 
690 1 0 |a SCANNING PROBE TECHNIQUES 
690 1 0 |a CARBON NANOTUBES 
700 1 |a Rubiolo, G.R. 
700 1 |a Salazar, A. 
700 1 |a Jimeno, A. 
700 1 |a Corcuera, M.A. 
700 1 |a Mondragon, Iñaki 
773 0 |d 2007  |g v. 16  |h pp. 412-417  |k n. 2  |p Diamond Relat. Mat.  |x 09259635  |w (AR-BaUEN)CENRE-4406  |t Diamond and Related Materials 
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856 4 0 |u https://doi.org/10.1016/j.diamond.2006.08.021  |y DOI 
856 4 0 |u https://hdl.handle.net/20.500.12110/paper_09259635_v16_n2_p412_Goyanes  |y Handle 
856 4 0 |u https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_09259635_v16_n2_p412_Goyanes  |y Registro en la Biblioteca Digital 
961 |a paper_09259635_v16_n2_p412_Goyanes  |b paper  |c PE 
962 |a info:eu-repo/semantics/article  |a info:ar-repo/semantics/artículo  |b info:eu-repo/semantics/publishedVersion 
999 |c 67694 

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