Use of an internal reference in 13C chemical shift measurements

The use of the nominal value of the chemical shift of the solvent to calibrate the spectrometer in 13C NMR spectroscopy was found to introduce errors due to the effect which the solute has on the solvent. In addition, hexamethyldisiloxane (HM) is proposed as an internal standard; owing to its high b...

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Autores principales: de Kowalewski, D.G., de Los Santos, C., Marceca, E.
Formato: JOUR
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Acceso en línea:http://hdl.handle.net/20.500.12110/paper_07491581_v28_n1_p1_deKowalewski
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