Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate

The investigation of the thermal behavior of calcium fructoborate samples of composition Ca(C<SUB>6</SUB>H<SUB>10</SUB>O<SUB>6</SUB>BO)<SUB>2</SUB>.3.5H<SUB>2</SUB>O showed that CaB<SUB>2</SUB>O<SUB>4</SUB> is genera...

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Detalles Bibliográficos
Autores principales:	Wagner, Claudia C., Barán, Enrique José
Formato:	Articulo
Lenguaje:	Inglés
Publicado:	2008
Materias:	Ingeniería Química Química calcium borate calcium fructoborate IR spectra high purity new synthetic procedure IR spectroscopy pyrolysis residue x ray analysis synthetic procedures thermal behaviors X-ray powder diffractometry pyrolysis
Acceso en línea:	http://sedici.unlp.edu.ar/handle/10915/38309 http://www.scielo.br/pdf/mr/v11n4/20.pdf
Aporte de:	SEDICI (UNLP) de Universidad Nacional de La Plata

Descripción
Sumario:	The investigation of the thermal behavior of calcium fructoborate samples of composition Ca(C<SUB>6</SUB>H<SUB>10</SUB>O<SUB>6</SUB>BO)<SUB>2</SUB>.3.5H<SUB>2</SUB>O showed that CaB<SUB>2</SUB>O<SUB>4</SUB> is generated as the final solid pyrolysis residue. On the basis of these observations a new, very easy, synthetic procedure for the preparation of high purity samples of this calcium borate is proposed. The material was characterized by X ray powder diffractometry and IR spectroscopy.